Practical
Getting the most out of a frit
Wash a new filter before first use. Fresh sintered glassware carries loose glass dust from manufacturing. Draw dilute hydrochloric acid through it, then rinse thoroughly with distilled water, before anything analytical goes near it.
Always clean by back-flushing. Push solvent through from the stem side, against the direction of filtration. Rinsing from the top drives the retained solids further into the channels, where they set hard and permanently reduce the flow rate.
Match the cleaning agent to the residue. There is no universal solvent for a blocked frit, and the wrong one can set the blockage permanently.
| Residue | Approach |
|---|
| Organic residues, greases and oils | A solvent the residue actually dissolves in, followed by acetone, then detergent and water. |
| Inorganic salts and mineral deposits | A warm dilute acid soak, then a thorough rinse with distilled water. |
| Stubborn or unidentified deposits | Time rather than force. A long soak clears far more than a stronger reagent, and costs you nothing if it fails. |
Never use hydrofluoric acid, hot phosphoric acid, or strong hot alkali on a frit. All three attack borosilicate glass itself. All three attack borosilicate glass itself. They widen the pores instead of clearing them, so the disc no longer matches its stated grade.